The other thing you should have set is the Windows 2000 sound control panel. It defaults to just a 2 speaker setting. If you have a 5.1 speaker setup then change the control panel to reflect it.
In the early stages of getting this setup going I'd advise on not using PowerDivx for now. Use BSPlayer and go into it's prefs and make sure you have it setup to use the SPDIF. Close the application, now go and double click the Wave Out registry hack that you downloaded from Dooms site. Now open BSPlayer back up and play your movie/AC3 file and it should work.
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